1.10
SciPi 770: Best Practices: Detecting and Quantifying Micro- Nanoplastics (MNP) in Biological Tissues
Is there a need for a field and procedural blank for every sampling?
Results
(9 Answers)
Most experts strongly agree that field and procedural blanks are necessary for every sampling, with 8 out of 9 experts answering "Yes." Experts cite several key reasons:
- Sampling conditions, weather, and airborne contamination can vary with each sampling (Expert 3)
- Blanks help identify potential contamination during sampling, transport, storage, and laboratory analysis (Expert 2)
- Microplastic analysis is particularly vulnerable to environmental contamination (Experts 1, 7)
- As microplastic analytical chemistry is still developing, comprehensive quality controls are essential (Expert 4)
The one dissenting expert (Expert 5) believes that multiple samples taken at the same place and time only require one field blank, suggesting a more pragmatic approach.
Expert 9 offers a middle ground, recommending blanks for every batch of samples rather than every individual sample, suggesting that approximately 10% of analyses should comprise quality control checks.
Summary Generated by AI
Answer Explanations
- Yes (please explain)Expert 3Ideally, yes. Sampling conditions, weather, airborne contamination, trip cross-contamination, all of these could very with each sampling, and such variation needs to be accounted for.
- Yes (please explain)Expert 9To clarify my response, I would recommend that these blank samples should be conducted for every batch of samples collected. The draft review recommends 10% of analyses should comprise such QC check samples (specifically blank and recovery checks). I think this is a reasonable and pragmatic approach.
- Yes (please explain)Expert 2Yes, in most of the cases, especially in the case of environmental sampling, pharmaceuticals, or analytical chemistry, both a field blank and a procedural (or lab) blank are necessary for each sampling event. These controls help ensure data integrity by identifying potential sources of contamination. A field blank is used to detect contamination that may occur during sampling, transport, or storage in the field, while a procedural blank is designed to reveal any contamination introduced during sample preparation and analysis in the laboratory. However, whether a blank is needed for every individual sample depends on the specific objectives of the study and the level of quality assurance required.
- Yes (please explain)Expert 4Especially as the analytical chemistry of MNP in most matrices is still in what can be considered its infancy, it is needed to include all kinds of blanks for every series of samples. Most likely, less blanks are needed when more information is obtained on the performance of such blanks over time.
- Yes (please explain)Expert 1One of the major sources of error in the analysis of MNPs is contamination from the environment. Field and procedural blanks help account for such contamination in the field or lab environment.
- NoExpert 5multiple samples taken at the same place and time only need one field blank.
- Yes (please explain)Expert 6Yes, it is necessary and useful to correct for human error and contamination.
- Yes (please explain)Expert 8absolutely, each field sampling campaign (if not day in the field) needs a field blank. The lab or procedural blank is needed one for each sample set that goes through the same procedure.
- Yes (please explain)Expert 7Field environment changes all the time and MNP can be introduced from ventilation and other sources and they are not constant.
Lab based contamination can happen with time also.
Expert 4
07/31/2025 03:00Expert 2
07/31/2025 07:04Expert 5
07/31/2025 11:50